Advertisement

Measurement Techniques

, Volume 62, Issue 7, pp 646–650 | Cite as

Investigation of Sorption Microsystems as Reference Samples of Volatile Organic Compounds

  • I. A. Platonov
  • I. N. KolesnichenkoEmail author
  • E. A. Novikova
  • L. V. Pavlova
Article
  • 10 Downloads

The technology of obtaining reference samples of volatile organic compounds using sorption microsystems is described. The most effective are 0.147–0.178 mm (80–100 mesh) polymer sorbents fractions, which provide high sorption properties, optimal gas-dynamic characteristics and minimal dead volumes. Stability of the reference samples during storage for 0.5 to 1 year is investigated. On the example of chamomile (Chamomilla recutita (L.)) growing in Samara region (Russia), it is shown that sorption microsystems can be used to identify complex objects and authenticate plant raw materials.

Keywords

sorption microsystems solid phase microextraction gas chromatography reference standards calibration gas mixtures 

Notes

This work was supported by the Russian Ministry of Education and Science in the framework of state assignment (Project No. 4.6875.2017/8.9).

References

  1. 1.
    M. Bodnar, J. Namieśnik, and P. Konieczka, “Validation of a sampling procedure,” Trends Analyt. Chem., No. 51, 117–126 (2013).CrossRefGoogle Scholar
  2. 2.
    G. C. Rhoderick, “The National Institute of Standards and Technology ambient level methane in air Standard Reference Material historical record,” Anal. Bioanal. Chem., 405, No. 1, 369 (2013).CrossRefGoogle Scholar
  3. 3.
    R. J. P. Grenfell, M. J. T. Milton, A. M. Harling, et al., “Standard mixtures of ambient volatile organic compounds in synthetic and whole air with stable reference values,” J. Geophys. Res. Atmos., 115, No. 14, 1 (2010).Google Scholar
  4. 4.
    Yu. A. Zolotov, “Some trends in modern analytical chemistry,” J. Chromatogr. Separ. Techn., 8, No. 2, 1–3 (2017).MathSciNetGoogle Scholar
  5. 5.
    K. Kuklinska, L. Wolska, and J. Namiesnik, “Air quality policy in the U.S. and the EU,” Atmos. Poll. Res., 6, No. 1, 129 (2015).CrossRefGoogle Scholar
  6. 6.
    Y. A. Kustikov and B. I. Popov, “Progress in development of Russian national measurement standards in the field of mass concentration measurement of suspended particles,” Mapan–J. Metrol. Soc. India, 28, No. 3, 181 (2013).Google Scholar
  7. 7.
    R. B. Shaevich, “Ensuring the correctness of the measurement results of small and ultrafine contents of components in substances, materials and media. Part 1. State of the problem,” Metrologiya, No. 3, 46–61 (2016).Google Scholar
  8. 8.
    I. A. Platonov, I. N. Kolesnichenko, E. A. Novikova, et al., “Preparation of calibration gas mixtures by the chromato-desorption method for improving the accuracy of quantitative determination of biogenic pentane in exhaled air,” Izmer. Tekhn., No. 8, 67–70 (2017).Google Scholar
  9. 9.
    Z. L. Baskin, “Support of the quality of environmental analytical control of air in industrial and living areas and flue-gas injection,” Zavod. Lab. Diagn. Mater., 68, No. 2, 45 (2002).ADSGoogle Scholar

Copyright information

© Springer Science+Business Media, LLC, part of Springer Nature 2019

Authors and Affiliations

  • I. A. Platonov
    • 1
  • I. N. Kolesnichenko
    • 1
    Email author
  • E. A. Novikova
    • 1
  • L. V. Pavlova
    • 1
  1. 1.Samara National Research UniversitySamaraRussia

Personalised recommendations