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Structural, Infrared, Magnetic, and Electrical Properties of Ni0.6Cd0.2Cu0.2Fe2O4 Ferrites Synthesized Using Sol-Gel Method Under Different Sintering Temperatures

  • Noura Kouki
  • Sobhi Hcini
  • Reema Aldawas
  • Michel Boudard
Original Paper
  • 12 Downloads

Abstract

Ni0.6Cd0.2Cu0.2Fe2O4 ferrites were synthesized using sol-gel method under different sintering temperatures. XRD patterns with the Rietveld refinement indicate that samples crystallize in the cubic spinel structure. The increase of sintering temperature leads successively to the increase of lattice constant, average crystallite size, intensities of absorption bands, magnetization, and electrical conductivity of the prepared ferrites. Dielectric constants decrease with frequency and their behaviors have been investigated using the interfacial polarization theory predicted by Maxwell. The modulus analysis shows the presence of electrical relaxation phenomenon and non-Debye nature for the samples. An appropriate electrical equivalent circuit was used to analyze the Nyquist plots, and the results show that the conduction mechanism of the synthesized ferrites is mainly due to the grain boundary contribution.

Keywords

Ferrites Sol-gel method Rietveld refinement Infrared properties, conductivity Dielectric properties 

Notes

Funding Information

This work was supported by the Deanship of Scientific Research at Al Qassim University under the research Project Number 5090-cosabu-2018-1-14-S.

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Copyright information

© Springer Science+Business Media, LLC, part of Springer Nature 2018

Authors and Affiliations

  • Noura Kouki
    • 1
    • 2
  • Sobhi Hcini
    • 3
  • Reema Aldawas
    • 1
  • Michel Boudard
    • 4
  1. 1.Department of Chemistry, College of Science and ArtsQassim UniversityBuraydahSaudi Arabia
  2. 2.Laboratory of Water, Technopole of Borj Cedria (CERTE)Membranes and Environment Biotechnology (EMBE)Hammam LifTunisia
  3. 3.Research Unit of Valorization and Optimization of Exploitation of Resources, Faculty of Science and Technology of Sidi BouzidUniversity of KairouanSidi BouzidTunisia
  4. 4.LMGP, CNRSUniversity of Grenoble AplesGrenobleFrance

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