Journal of Superconductivity and Novel Magnetism

, Volume 32, Issue 2, pp 145–150 | Cite as

Critical Current Density and AC Susceptibility of Bi1.6Pb0.4Sr2Ca2Cu3O10 Superconductor with Ni0.5Zn0.5Fe2O4 Nanomaterial

  • Nurul Raihan Mohd Suib
  • Ilhamsyah Putra Abu Bakar
  • N. B. Ibrahim
  • R. Abd-ShukorEmail author
Original Research


The juxtaposition of superconductivity and magnetism is an interesting research topic due to the exclusivity nature of both phenomena. In this paper, we report the effect of nanosized (~ 5 nm) nickel zinc ferrite Ni0.5Zn0.5Fe2O4 (NZFO) on Bi1.6Pb0.4Sr2Ca2Cu3O10 (Bi-2223) superconductor. Bi-2223 powders were prepared using the co-precipitation method. Samples with starting formula Bi1.6Pb0.4Sr2Ca2Cu3O10(Ni0.5Zn0.5Fe2O4)x for x = 0 to 0.1 wt% have been prepared. The structure, microstructure, electrical resistance, and AC susceptibility were determined. The transport critical current density, Jct, was measured using the 1 μV/cm criterion. The non-added sample sintered for 48 h showed the highest zero resistance temperature, Tc-zero (105 K) and Jct of 1.83 A cm−2 at 40 K. The x = 0.02 wt% sample sintered for 48 h (Tc-zero = 103 K) showed the highest Jct of 5.30 A cm−2 at 40 K. The peak temperature of the imaginary part of the complex susceptibility, Tp, increased with sintering time and nanoparticle addition, indicating full flux penetration occurred at higher temperatures and improved intergrain coupling. NZFO nanoparticle did not suppress the transition temperature but it improved the transport critical current density by more than five times indicating it enhanced flux pinning and connectivity between grains in the Bi-2223 phase.


Superparamagnetism Transport current Grain coupling Flux pinning 


Funding Information

This research was supported by the Ministry of Education, Malaysia under grant no. FRGS/1/2017/STG02/UKM/01/1.

Compliance with Ethical Standards

Conflict of Interest

The authors declare that they have no conflict of interest.


  1. 1.
    Kong, W., Abd-Shukor, R.: J. Supercond. Nov. Mag. 23, 257 (2009)CrossRefGoogle Scholar
  2. 2.
    Hafiz, M., Abd-Shukor, R.: Adv Mat Sci Engg. Art. No. 146476. (2015)Google Scholar
  3. 3.
    Roumié, M., Marhaba, S., Awad, R., Kork, M., Hassan, I., Mawassi, R.: J. Supercond. Nov. Mag. 27, 143 (2013)CrossRefGoogle Scholar
  4. 4.
    Agail, A., Abd-Shukor, R.: J. Supercond. Nov. Mag. 27, 1273 (2014)CrossRefGoogle Scholar
  5. 5.
    Kong, W., Abd-Shukor, R.: J. Elect. Mat. 36(12), 1648 (2007)ADSCrossRefGoogle Scholar
  6. 6.
    Barakat, M.M.E., Isber, S., Al-Sayyed, N., Awad, R., Roumié, M.: J. Supercond. Nov. Mag. 29(7), 1703 (2016)CrossRefGoogle Scholar
  7. 7.
    Muhammad-Aizat, K., Abd-Shukor, R.: Sains Malays. 47(7), 1579 (2018)CrossRefGoogle Scholar
  8. 8.
    Lyuksyutov, I.F., Naugle, D.G.: Mod. Phys. Lett. B. 13, 491 (1999)ADSCrossRefGoogle Scholar
  9. 9.
    Gul, I.H., Amin, F., Abbasi, A.Z., Anis-ur-Rehman, M., Maqsood, A.: Phys. C. 449(2), 139 (2006)ADSCrossRefGoogle Scholar
  10. 10.
    Zhang, W., Ramesh, R., MacManus-Driscoll, J.L., Wang, H.: MRS Bull. 40(9), 736 (2015)CrossRefGoogle Scholar
  11. 11.
    Morrison, S.A., Cahill, C.L., Carpenter, E.E., Calvin, S., Swaminathan, R., McHenry, M.E., Harris, V.G.: J. Appl. Phys. 95, 6392 (2004)ADSCrossRefGoogle Scholar
  12. 12.
    Chen, D.G., Tang, X.G., Tong, J.J., Wu, J.B., Jiang, Y.P., Liu, Q.X.: Solid State Commun. 151, 1042 (2011)ADSCrossRefGoogle Scholar
  13. 13.
    Yu, Q.Y., Liu, H.K., Dou, S.X.: Phys. C. 250, 7–14 (1995)ADSCrossRefGoogle Scholar
  14. 14.
    Nkum, R.K., Datars, W.R.: Supercond. Sci. Technol. 8, 822–826 (1995)ADSCrossRefGoogle Scholar
  15. 15.
    Bean, C.P.: Rev. Mod. Phys. 36, 31 (1964)ADSCrossRefGoogle Scholar
  16. 16.
    Gomory, F.: Supercond. Sci. Technol. 10, 523 (1997)ADSCrossRefGoogle Scholar
  17. 17.
    Nabil, A.A.: Yahya, Abd-Shukor, R. J. Supercond. Nov. Mag. 27(2), 329 (2014)CrossRefGoogle Scholar
  18. 18.
    Agail, A., Abd-Shukor, R.: Appl. Phys. A Mater. Sci. Process. 112(2), 501 (2013)ADSCrossRefGoogle Scholar
  19. 19.
    Azman, N.J., Abdullah, H., Abd-Shukor, R.: Adv. Cond. Mat. Phys. Art. No. 498747 (2014)Google Scholar
  20. 20.
    Kilic, A., Kilic, K., Senoussi, S.: J. Appl. Phys. 84(6), 3254 (1998)ADSCrossRefGoogle Scholar
  21. 21.
    Kilic, A.: Supercond. Sci. Technol. 8, 497 (1995)ADSCrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media, LLC, part of Springer Nature 2018

Authors and Affiliations

  • Nurul Raihan Mohd Suib
    • 1
    • 2
    • 3
  • Ilhamsyah Putra Abu Bakar
    • 1
  • N. B. Ibrahim
    • 1
  • R. Abd-Shukor
    • 1
    Email author
  1. 1.School of Applied PhysicsUniversiti Kebangsaan MalaysiaBangiMalaysia
  2. 2.Faculty of Applied SciencesUniversiti Teknologi MARAShah AlamMalaysia
  3. 3.Pusat Asasi UiTM Kampus DengkilUniversiti Teknologi MARADengkilMalaysia

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