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Surfactant-assisted imidacloprid intercalation of layered zinc hydroxide nitrate: synthesis, characterisation and controlled release formulation

  • Sharifah Norain Mohd Sharif
  • Norhayati HashimEmail author
  • Illyas Md Isa
  • Suriani Abu Bakar
  • Mohamad Idris Saidin
  • Mohamad Syahrizal Ahmad
  • Mazidah Mamat
  • Mohd Zobir Hussein
Article
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Abstract

A neutrally charged insecticide, imidacloprid (IC), has been intercalated into zinc hydroxide nitrate (ZHN) with the assistance of sodium dodecylsulphate (SDS). The presence of SDS assists the intercalation of IC by forming a hydrophobic region in the interlayer gallery of ZHN. The intercalated compound, ZHN–SDS–IC, was characterised using powder X-ray diffraction (PXRD), thermogravimetric analysis, Fourier transform infrared spectroscopy, elemental analysis, field emission scanning electron microscopy, and gas sorption analysis. The PXRD studies demonstrated intercalation peaks at lower 2θ, which confirmed the intercalation of IC and SDS in the interlayer gallery of ZHN. The release and kinetic studies of ZHN–SDS–IC reveals that the IC were successfully released in controlled manner (with release time up to 1478 min), and were governed by pseudo second order kinetic model. The ZHN–SDS–IC synthesised is hopefully beneficial in overcoming the consequences of excessive usage of insecticide in paddy cultivation.

Keywords

Imidacloprid Zinc hydroxide nitrate Intercalation Sodium dodecylsulphate Controlled release formulation 

Notes

Acknowledgements

The authors wish to thank UPSI and the Ministry of Education Malaysia for supporting this research. This work was supported by the GPU-RISING STAR Grant No. 2019 − 0119 − 103 − 01.

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Copyright information

© Springer Science+Business Media, LLC, part of Springer Nature 2019

Authors and Affiliations

  • Sharifah Norain Mohd Sharif
    • 1
  • Norhayati Hashim
    • 1
    • 2
    Email author
  • Illyas Md Isa
    • 1
    • 2
  • Suriani Abu Bakar
    • 2
    • 3
  • Mohamad Idris Saidin
    • 1
  • Mohamad Syahrizal Ahmad
    • 1
  • Mazidah Mamat
    • 4
  • Mohd Zobir Hussein
    • 5
  1. 1.Department of Chemistry, Faculty of Science and MathematicsUniversiti Pendidikan Sultan IdrisTanjong MalimMalaysia
  2. 2.Nanotechnology Research Centre, Faculty of Science and MathematicsUniversiti Pendidikan Sultan IdrisTanjong MalimMalaysia
  3. 3.Department of Physics, Faculty of Science and MathematicsUniversiti Pendidikan Sultan IdrisTanjong MalimMalaysia
  4. 4.School of Fundamental ScienceUniversiti Malaysia TerengganuKuala TerengganuMalaysia
  5. 5.Materials Synthesis and Characterization Laboratory, Institute of Advanced TechnologyUniversiti Putra MalaysiaSerdangMalaysia

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