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Journal of Materials Science

, Volume 54, Issue 8, pp 6594–6607 | Cite as

Strain-rate-dependent deformation behaviour of high-carbon steel in compression: mechanical and structural characterisation

  • Amborish BanerjeeEmail author
  • Rumana Hossain
  • Farshid Pahlevani
  • Qiang Zhu
  • Veena Sahajwalla
  • B. Gangadhara Prusty
Metals
  • 200 Downloads

Abstract

Dual-phase high-carbon steels are of significant interest in mining industries particularly in comminution and rock handling applications where the strain rate varies from very low to very high. The effect of quasi-static strain rate on the deformation behaviour of austenite–martensite high-carbon low-alloy steel is investigated for compression loading in this paper. Experiments were conducted at different compressive strain rates (2.56 × 10−4 to 2.56 × 10−1 s−1), and the subsequent microstructural evolution was characterised by optical microscopy, X-ray diffraction (XRD), scanning electron microscopy and electron backscatter diffraction (EBSD) techniques to establish the structure–property correlation. The experimental results indicated an increase in the yield strength (σy) with the increase in the strain rate due to the rate-dependent dislocation velocities. The strain hardening rate of the material exhibited a decreasing trend with an increase in the true strain values for all the applied strain rates. XRD results indicated the phenomenon of deformation-induced martensitic transformation (DIMT) to be rate dependent, whereas EBSD results showed an increase in the Kernel average misorientation values with increase in the strain rate. The volume fraction of retained austenite was observed to be decreasing with an increase in the engineering strain values irrespective of the applied strain rate. The microscopic features of the fracture surfaces showed the presence of transgranular cracking at low strain rates, whereas predominant intergranular cracks were found at higher strain rates. TEM results indicated the decrease in the lath martensites with increase in the strain rate.

Notes

Acknowledgements

The work was supported under the Australian Research Council’s Industrial Transformation Research Hub (ARC-ITRH) funding scheme (IH130200025). The authors acknowledge the technical support and assistance provided by the Australian Microscopy and Microanalysis Research Facility at Mark Wainwright Analytical Centre, UNSW Sydney.

Compliance with ethical standards

Conflict of interest

The authors declare that they have no conflict of interest.

References

  1. 1.
    Tavares SSM, Mello SR, Gomes AM, Neto JM, da Silva MR, Pardal JM (2006) X-ray diffraction and magnetic characterization of the retained austenite in a chromium alloyed high carbon steel. J Mater Sci 41(15):4732–4736.  https://doi.org/10.1007/s10853-006-0025-8 CrossRefGoogle Scholar
  2. 2.
    Hossain R, Pahlevani F, Witteveen E, Banerjee A, Joe B, Prusty BG, Dippenaar R, Sahajwalla V (2017) Hybrid structure of white layer in high carbon steel: formation mechanism and its properties. Sci Rep 7(1):13288CrossRefGoogle Scholar
  3. 3.
    Ogawa T, Koyama M, Tasan CC, Tsuzaki K, Noguchi H (2017) Effects of martensitic transformability and dynamic strain age hardenability on plasticity in metastable austenitic steels containing carbon. J Mater Sci 52(13):7868–7882.  https://doi.org/10.1007/s10853-017-1052-3 CrossRefGoogle Scholar
  4. 4.
    Manjanna J, Kobayashi S, Kamada Y, Takahashi S, Kikuchi H (2008) Martensitic transformation in SUS 316LN austenitic stainless steel at RT. J Mater Sci 43(8):2659–2665.  https://doi.org/10.1007/s10853-008-2494-4 CrossRefGoogle Scholar
  5. 5.
    Yang X-S, Sun S, Zhang T-Y (2015) The mechanism of bcc α′ nucleation in single hcp ε laths in the fcc γ → hcp ε → bcc α′ martensitic phase transformation. Acta Mater 95:264–273CrossRefGoogle Scholar
  6. 6.
    Xie L, Huang T-L, Wang Y-H, Wu G-L, Tsuji N, Huang X-X (2017) Deformation induced martensitic transformation and its initial microstructure dependence in a high alloyed duplex stainless steel. Steel Res Int 88:1700169CrossRefGoogle Scholar
  7. 7.
    Nagy E, Mertinger V, Tranta F, Sólyom J (2004) Deformation induced martensitic transformation in stainless steels. Mater Sci Eng A 378(1):308–313CrossRefGoogle Scholar
  8. 8.
    Seol J-B, Jung JE, Jang YW, Park CG (2013) Influence of carbon content on the microstructure, martensitic transformation and mechanical properties in austenite/ε-martensite dual-phase Fe–Mn–C steels. Acta Mater 61(2):558–578CrossRefGoogle Scholar
  9. 9.
    Choi HC, Ha TK, Shin HC, Chang YW (1999) The formation kinetics of deformation twin and deformation induced ε-martensite in an austenitic Fe–C–Mn steel. Scripta Mater 40(10):1171–1177CrossRefGoogle Scholar
  10. 10.
    Dagbert C, Sehili M, Gregoire P, Galland J, Hyspecka L (1996) Mechanical study of instability of austenitic FeNiC alloys: effect of hydrogen. Acta Mater 44(7):2643–2650CrossRefGoogle Scholar
  11. 11.
    Nakada N, Ito H, Matsuoka Y, Tsuchiyama T, Takaki S (2010) Deformation-induced martensitic transformation behavior in cold-rolled and cold-drawn type 316 stainless steels. Acta Mater 58(3):895–903CrossRefGoogle Scholar
  12. 12.
    Solomon N, Solomon I (2017) Effect of deformation-induced phase transformation on AISI 316 stainless steel corrosion resistance. Eng Fail Anal 79(Supplement C):865–875CrossRefGoogle Scholar
  13. 13.
    Kireeva IV, Chumlyakov YI (2008) The orientation dependence of γ–α′ martensitic transformation in austenitic stainless steel single crystals with low stacking fault energy. Mater Sci Eng A 481(Supplement C):737–741CrossRefGoogle Scholar
  14. 14.
    Ishida K (1976) Direct estimation of stacking fault energy by thermodynamic analysis. Phys Status Solidi A 36(2):717–728CrossRefGoogle Scholar
  15. 15.
    Varma SK, Kalyanam J, Murk LE, Srinivas V (1994) Effect of grain size on deformation-induced martensite formation in 304 and 316 stainless steels during room temperature tensile testing. J Mater Sci Lett 13(2):107–111CrossRefGoogle Scholar
  16. 16.
    Sadeghpour S, Kermanpur A, Najafizadeh A (2014) Investigation of the effect of grain size on the strain-induced martensitic transformation in a high-Mn stainless steel using nanoindentation. Mater Sci Eng A 612(Supplement C):214–216CrossRefGoogle Scholar
  17. 17.
    Li Q, Wang T, Li H, Gao Y, Li N, Jing T (2010) Warm deformation behavior of steels containing carbon of 0.45% to 1.26% with martensite starting structure. J Iron Steel Res Int 17(5):34–37CrossRefGoogle Scholar
  18. 18.
    Wray PJ (1982) Effect of carbon content on the plastic flow of plain carbon steels at elevated temperatures. Metall Trans A 13(1):125–134CrossRefGoogle Scholar
  19. 19.
    Serajzadeh S, Taheri AK (2003) An investigation into the effect of carbon on the kinetics of dynamic restoration and flow behavior of carbon steels. Mech Mater 35(7):653–660CrossRefGoogle Scholar
  20. 20.
    Lee W-S, Liu C-Y (2006) The effects of temperature and strain rate on the dynamic flow behaviour of different steels. Mater Sci Eng A 426(1–2):101–113CrossRefGoogle Scholar
  21. 21.
    Moshksar MM, Marzban Rad E (1998) Effect of temperature and strain rate on the superplastic behaviour of high-carbon steel. J Mater Process Technol 83(1–3):115–120CrossRefGoogle Scholar
  22. 22.
    Liu ZG, Fecht HJ, Xu Y, Yin J, Tsuchiya K, Umemoto M (2003) Electron-microscopy investigation on nanocrystal formation in pure Fe and carbon steel during ball milling. Mater Sci Eng A 362(1–2):322–326CrossRefGoogle Scholar
  23. 23.
    Saeidi F, Yahyaei M, Powell M, Tavares LM (2017) Investigating the effect of applied strain rate in a single breakage event. Miner Eng 100:211–222CrossRefGoogle Scholar
  24. 24.
    Suryanarayana C (2001) Mechanical alloying and milling. Prog Mater Sci 46(1–2):1–184CrossRefGoogle Scholar
  25. 25.
    Standard Test Methods of Compression Testing of Metallic Materials at Room Temperature. ASTM International, ASTM E9-09, West Conshohocken (2009)Google Scholar
  26. 26.
    Paupler P, Dieter GE (1988) Mechanical metallurgy. 3rd ed., Mc Graw-Hill Book Co., New York 1986. XXIII + 751 p., DM 138.50, ISBN 0-07-016893-8. Cryst Res Technol 23(2):194CrossRefGoogle Scholar
  27. 27.
    Hull D, Bacon DJ (2011) Chapter 3: Movement of dislocations. In: Hull D, Bacon DJ (eds) Introduction to dislocations, 5th edn. Butterworth-Heinemann, Oxford, pp 43–62CrossRefGoogle Scholar
  28. 28.
    Ma X, Li F, Cao J, Li J, Sun Z, Zhu G, Zhou S (2018) Strain rate effects on tensile deformation behaviors of Ti–10V–2Fe–3Al alloy undergoing stress-induced martensitic transformation. Mater Sci Eng A 710:1–9CrossRefGoogle Scholar
  29. 29.
    Tahreen N, Chen DL, Nouri M, Li DY (2014) Effects of aluminum content and strain rate on strain hardening behavior of cast magnesium alloys during compression. Mater Sci Eng A 594:235–245CrossRefGoogle Scholar
  30. 30.
    Banerjee A, Prusty BG, Bhattacharyya S (2019) Rate-dependent mechanical strength and flow behaviour of dual-phase high carbon steel at elevated temperatures: an experimental investigation. Mater Sci Eng A 744:224–234CrossRefGoogle Scholar
  31. 31.
    Yang HK, Zhang ZJ, Dong FY, Duan QQ, Zhang ZF (2014) Strain rate effects on tensile deformation behaviors for Fe–22Mn–0.6C–(1.5Al) twinning-induced plasticity steel. Mater Sci Eng A 607:551–558CrossRefGoogle Scholar
  32. 32.
    Sahu P, Shee SK, Hamada AS, Rovatti L, Sahu T, Mahato B, Ghosh Chowdhury S, Porter DA, Karjalainen LP (2012) Low strain rate deformation behavior of a Cr–Mn austenitic steel at −80°C. Acta Mater 60(20):6907–6919CrossRefGoogle Scholar
  33. 33.
    Polat A (2012) The effects of strain rate and temperature on the deformation behavior of cold-rolled TRIP800 steel. Steel Res Int 83(8):775–782CrossRefGoogle Scholar
  34. 34.
    Park WS, Yoo SW, Kim MH, Lee JM (2010) Strain-rate effects on the mechanical behavior of the AISI 300 series of austenitic stainless steel under cryogenic environments. Mater Des 31(8):3630–3640CrossRefGoogle Scholar
  35. 35.
    Tiamiyu AA, Eskandari M, Nezakat M, Wang X, Szpunar JA, Odeshi AG (2016) A comparative study of the compressive behaviour of AISI 321 austenitic stainless steel under quasi-static and dynamic shock loading. Mater Des 112:309–319CrossRefGoogle Scholar
  36. 36.
    Tiamiyu AA, Odeshi AG, Szpunar JA (2018) Multiple strengthening sources and adiabatic shear banding during high strain-rate deformation of AISI 321 austenitic stainless steel: effects of grain size and strain rate. Mater Sci Eng A 711:233–249CrossRefGoogle Scholar
  37. 37.
    Hossain R, Pahlevani F, Quadir MZ, Sahajwalla V (2016) Stability of retained austenite in high carbon steel under compressive stress: an investigation from macro to nano scale. Sci Rep 6:34958CrossRefGoogle Scholar
  38. 38.
    Saeidi N, Ashrafizadeh F, Niroumand B, Barlat F (2014) Evaluation of fracture micromechanisms in a fine-grained dual phase steel during uniaxial tensile deformation. Steel Res Int 85(9):1386–1392CrossRefGoogle Scholar
  39. 39.
    Liu YG, Li MQ (2018) Characteristics of martensite transformed from deformed austenite with various states of ultrahigh strength 300 M steel. Mater Charact 144:490–497CrossRefGoogle Scholar
  40. 40.
    Guimarães JRC, Rios PR (2015) Microstructural path analysis of martensite dimensions in FeNiC and FeC alloys. Mater Res 18:595–601CrossRefGoogle Scholar
  41. 41.
    Zhang M, Wang YH, Zheng CL, Zhang FC, Wang TS (2014) Austenite deformation behavior and the effect of ausforming process on martensite starting temperature and ausformed martensite microstructure in medium-carbon Si–Al-rich alloy steel. Mater Sci Eng A 596:9–14CrossRefGoogle Scholar
  42. 42.
    Shen YF, Li XX, Sun X, Wang YD, Zuo L (2012) Twinning and martensite in a 304 austenitic stainless steel. Mater Sci Eng A 552(Supplement C):514–522CrossRefGoogle Scholar
  43. 43.
    Kochmann DM, Le KC (2009) A continuum model for initiation and evolution of deformation twinning. J Mech Phys Solids 57(6):987–1002CrossRefGoogle Scholar
  44. 44.
    Steinmetz DR, Jäpel T, Wietbrock B, Eisenlohr P, Gutierrez-Urrutia I, Saeed-Akbari A, Hickel T, Roters F, Raabe D (2013) Revealing the strain-hardening behavior of twinning-induced plasticity steels: theory, simulations, experiments. Acta Mater 61(2):494–510CrossRefGoogle Scholar
  45. 45.
    Canadinc D, Efstathiou C, Sehitoglu H (2008) On the negative strain rate sensitivity of Hadfield steel. Scripta Mater 59(10):1103–1106CrossRefGoogle Scholar

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© Springer Science+Business Media, LLC, part of Springer Nature 2019

Authors and Affiliations

  1. 1.School of Mechanical and Manufacturing EngineeringUNSW SydneySydneyAustralia
  2. 2.Centre for Sustainable Materials Research and Technology, School of Materials Science and EngineeringUNSW SydneySydneyAustralia
  3. 3.Electron Microscopy UnitMark Wainwright Analytical CentreSydneyAustralia

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