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Journal of Materials Science

, Volume 44, Issue 16, pp 4407–4412 | Cite as

Synthesis of Fe3O4 polyhedra by hydrothermal method: using l-arginine as precipitator

  • Lianfeng Duan
  • Shusheng Jia
  • Yanjun Wang
  • Jian Chen
  • Lijun ZhaoEmail author
Article

Abstract

Unusual polyhedral structures of cubic Fe3O4 were fabricated in high yield via a facile hydrothermal method in the presence of a surfactant cetyltrimethyammonium bromide (CTAB). Hexagonal, dodecahedral, truncated octahedral, and octahedral shapes can be prepared by changing the concentration of the CTAB in l-arginine solutions. In the solution-phase synthesis, both the l-arginine and CTAB were found to be the prime factors for the formation of the polyhedral structures. In addition, room-temperature vibrating sample magnetometer (VSM) testing results indicated that the magnetite synthesized without the addition of CTAB had the highest Ms value and the lowest Hc value. This synthesis method is also suitable for the preparation of other ferrites with spinel structure.

Keywords

Ferrite Magnetite CTAB HRTEM Vibrate Sample Magnetometer 

Notes

Acknowledgements

This study was supported by the Basic Research Expenses for the Special Funds of Jilin University.

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Copyright information

© Springer Science+Business Media, LLC 2009

Authors and Affiliations

  • Lianfeng Duan
    • 1
  • Shusheng Jia
    • 1
  • Yanjun Wang
    • 2
  • Jian Chen
    • 1
  • Lijun Zhao
    • 1
    Email author
  1. 1.Key Laboratory of Automobile Materials, Ministry of Education and Department of Materials Science and EngineeringJilin UniversityChangchunPeople’s Republic of China
  2. 2.The Second Hospital of Jilin UniversityChangchunPeople’s Republic of China

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