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Glass and Ceramics

, Volume 76, Issue 1–2, pp 7–10 | Cite as

Synthesis Temperature Influence on the AlMgB14 Phase Composition

  • D. D. NesmelovEmail author
  • D. P. Danilovich
  • S. N. Perevislov
  • S. S. Ordan’yan
SCIENCE FOR CERAMIC PRODUCTION
  • 13 Downloads

The influence of the synthesis temperature on the phase composition, size distribution, and morphology of AlMgB14 particles, obtained by direct interaction of powders of elementary Al, Mg, and B with the addition of free carbon in vacuum 10 – 2 Pa at 1200 – 1400°C, was studied. The synthesized powders were analyzed by means of x-ray diffraction, SEM, EDX, and laser diffraction. The highest mass content of the main phase AlMgB14 (94%) was obtained at synthesis temperature 1200 – 1300°C with 1 h soaking. Impurity MgAl2O4 as well as magnesium-depleted spinel and AlB12 were recorded at soaking temperature above 1300°C.

Keywords

aluminum-magnesium boride synthesis light-density borides phase composition particle-size distribution nano-size powder 

Notes

This work was supported by RFBR (contract No. 17-03-00863 A) and was performed using equipment from the Engineering Center at the St. Petersburg State Institute of Technology (Technological University).

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Copyright information

© Springer Science+Business Media, LLC, part of Springer Nature 2019

Authors and Affiliations

  • D. D. Nesmelov
    • 1
    Email author
  • D. P. Danilovich
    • 1
  • S. N. Perevislov
    • 2
  • S. S. Ordan’yan
    • 1
  1. 1.St. Petersburg State Technological Institute (Technical University)St. PetersburgRussia
  2. 2.I. V. Grebenshchikov Institute of Silicate ChemistrySt. PetersburgRussia

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