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Organophosphorus derivatives of α-chlorothiophene

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Conclusions

  1. 1.

    α-Chlorothienyldichlorophosphine was obtained by the reaction ofα-chlorothiophene was phosphorus trichloride in the presence of SnCl4.

  2. 2.

    α-Chlorothienyldichlorophosphine is alkylated by tetraethyllead at the phosphorus atom to give ethyl-α-chlorothienylchlorophosphine.

  3. 3.

    A study was made of the reaction of ethyl-α-chlorothienylehlorophosphine with alcohol, diethylamine, acrylic acid, acrylamide, and methacrylamide.

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Literature cited

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    M. Bentov, L. David, and E. D. Bergmann, J. Chem. Soc., 4750 (1964).

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    E. L. Gefter, Zh. Obshch. Khim.,28, 1338 (1958).

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    J. F. Allen and O. H. Johnson, J. Amer. Chem. Soc.,77, 2871 (1955).

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    F. W. Lichtenthaler, Chem. Rev.,61, 607 (1961).

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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 8, pp. 1846–1849, August, 1974.

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Khairullin, V.K., Nesterenko, L.I., Savushkina, V.I. et al. Organophosphorus derivatives of α-chlorothiophene. Russ Chem Bull 23, 1765–1768 (1974). https://doi.org/10.1007/BF00923207

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Keywords

  • Alcohol
  • Phosphorus
  • Acrylamide
  • Acrylic Acid
  • SnCl4