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Reactions of chlorides, some esters, and amides of γ-chloropropylphosphonic and bis-(γ-chloropropyl)phosphinic acid with amines

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Conclusions

  1. 1.

    The reactions ofγ-chloropropylphosphonic and bis(γ-chloropropyl)phosphinic acid chlorides with amines have been studied.

  2. 2.

    The reaction of diethylamine with esters and amides ofγ-chloropropylphosphonic and bis(γ-chloropropyl)phosphinic acids gave the derivatives of N-diethylaminopropylphosphonic and bis(N,N-diethylaminopropyl)phosphinic acids.

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Literature cited

  1. 1.

    G. M. Vinokurova and I. A. Aleksandrova, Izv. Akad. Nauk SSSR, Ser. Khim.,1969, 884.

  2. 2.

    G. Kosolapoff, J. Amer. Chem. Soc.,63, 2112 (1947).

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    K. A. Petrov, A. I. Gavrilova, and V. P. Korotkova, Zh. Obshch. Khim.,32, 915 (1962).

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    M. I. Kabachnik and T. Ya. Medved', Izv. Akad. Nauk SSSR, Otd. Khim. Nauk,1950, 635.

  5. 5.

    L. Bellamy, Infrared Spectra of Complex Molecules [Russian translation], IL (1963), p. 415.

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    R. R. Shagidullin and N. P. Grechkin, Chemistry and Applications of Organophosphorus Compounds, Izd. Akad. Nauk SSSR (1962), p. 112.

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Additional information

Translated from Izvestiya Akademii Nauk, SSSR, Seriya Khimicheskaya, No. 5, pp. 1163–1166, May, 1969.

The authors acknowledge R. R. Shagidullin's valuable advice and help in the interpretation of IR spectra.

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Aleksandrova, I.A., Vinokurova, G.M. Reactions of chlorides, some esters, and amides of γ-chloropropylphosphonic and bis-(γ-chloropropyl)phosphinic acid with amines. Russ Chem Bull 18, 1064–1066 (1969). https://doi.org/10.1007/BF00922874

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Keywords

  • Chloride
  • Ester
  • Amide
  • Acid Chloride
  • Diethylamine