The reactions ofγ-chloropropylphosphonic and bis(γ-chloropropyl)phosphinic acid chlorides with amines have been studied.
The reaction of diethylamine with esters and amides ofγ-chloropropylphosphonic and bis(γ-chloropropyl)phosphinic acids gave the derivatives of N-diethylaminopropylphosphonic and bis(N,N-diethylaminopropyl)phosphinic acids.
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G. M. Vinokurova and I. A. Aleksandrova, Izv. Akad. Nauk SSSR, Ser. Khim.,1969, 884.
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Translated from Izvestiya Akademii Nauk, SSSR, Seriya Khimicheskaya, No. 5, pp. 1163–1166, May, 1969.
The authors acknowledge R. R. Shagidullin's valuable advice and help in the interpretation of IR spectra.
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Aleksandrova, I.A., Vinokurova, G.M. Reactions of chlorides, some esters, and amides of γ-chloropropylphosphonic and bis-(γ-chloropropyl)phosphinic acid with amines. Russ Chem Bull 18, 1064–1066 (1969). https://doi.org/10.1007/BF00922874
- Acid Chloride