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Evaluation of the purity of isomers of 1-oxo-1-chlorophospholenes and determination of the compositions of their mixtures

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Summary

  1. 1.

    The purity of 1-oxo-1-chlorophospholene-2 and 1-oxo-1-chlorophospholene-3 have been determined spectrally.

  2. 2.

    A method is suggested for the evaluation of the composition of their mixtures from the relative intensities of the δ5CH2 absorption bands in the IR spectra.

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Literature cited

  1. 1.

    B.A. Arbuzov, A.O. Vizel', O.A. Raevskii, Yu.F. Tarenko, and D. F. Fazliev, Izv. Akad. Nauk SSSR, Ser. Khim., 1882 (1968).

  2. 2.

    B.A. Arbuzov, A.O. Vizel', Yu.Yu. Samitov, and Yu.F. Tarenko, Izv. Akad. Nauk SSSR, Ser. Khim., 672 (1967).

  3. 3.

    K Hunger, U. Hasserodt, and F. Korte, Tetrahedron,20, 1593 (1964).

  4. 4.

    L. Bellamy, Infrared Spectra of Complex Molecules [Russian translation], IL (1963), p. 34.

  5. 5.

    C.N. Rao, Chemical Applications of Infrared Spectroscopy, Academic Press, New York-London (1963), p. 138.

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Additional information

Translated rom Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 2, pp. 460–462, February, 1969.

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Arbuzov, B.A., Vizel', A.O., Raevskii, O.A. et al. Evaluation of the purity of isomers of 1-oxo-1-chlorophospholenes and determination of the compositions of their mixtures. Russ Chem Bull 18, 408–410 (1969). https://doi.org/10.1007/BF00905565

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Keywords

  • Absorption Band
  • Relative Intensity