The previously undescribed N-2-hydroxyethylcrotonamide and N-2-hydroxyethyl-N-methylcrotonarnide were synthesized and characterized. N-2-Hydroxyethylcrotonamide was prepared by the reaction of crotonyl chloride and 2-aminoethanol in chloroform. N-2-Hydroxyethyl-N-methylcrotonamide was prepared by the reaction of crotonyl chloride and 2-methylaminoethanol in an aqueous solution of alkali.
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S. N. Ushakov, E. M. Lavrent'eva, and K. S. Podgorskaya, Izv. AN SSSR. Otd. khim, n. 1959, 91.
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Beilsteins Handbuch d. Organ. Chem, Fierté Auflage, Berlin.
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Ushakov, S.N., Aleev, K.M. Synthesis of n-2-hydroxyethylcrotonamide and n-2-hydroxyethyl-n-methylcrotonamide. Russ Chem Bull 11, 641–642 (1962). https://doi.org/10.1007/BF00904767
- Aqueous Solution
- Crotonyl Chloride