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Preparative gas-liquid chromatography with increased efficiency

Conclusions

  1. 1.

    The optimum conditions for the preparative gas-chromatographic separation of organic substances with an efficiency of up to 2000 theoretical plates, with a simultaneous load of up to 1–2 g, were developed.

  2. 2.

    Designs of an accessible preparative chromatograph for the separation of unstable compounds were suggested, and the possibility of using it for the separation of organic substances of various classes was demonstrated.

  3. 3.

    The promise of the use of sodium chloride as the solid phase for the preparative gas-chromatographic separation of unstable compounds was demonstrated.

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Literature cited

  1. 1.

    K.V. Alekseeva, V.G. Berzkin, S.A. Volkov, and E.G. Rastyannikov, Analytical and Comparative Surveys [in Russian], No. 2, TsNIITÉNeftekhim (1968).

  2. 2.

    B.A. Kazanskii, E.A. Mikhailova, and A.I. D'yachenko, Transactions of the Second All-Union Conference [in Russian], Moscow (March 17, 1962), p. 223.

  3. 3.

    F.A. Huyten, W. von Beersom, and G.W.A. Rijndres, Gas Chromatography, Proc. of the Third Symposium (1960), R.P.W. Scott (editor), Butterworths, London (1960), p. 224.

  4. 4.

    G.I. Frisone, J. Chromatogr.,6, 97 (1961).

  5. 5.

    E. Bayer, Gas Chromatography, Proc. of the Third Symposium (1960), R.P.W. Scott (editor), Butterworths, London (1960), p. 240.

  6. 6.

    U.D. de Vem and V. Pretorius, Gas-Liquid Chromatography [Russian translation], No. 2, NIITÉKhim (1963), p. 61.

  7. 7.

    U. Takeda, Reports. Govt. Chem. Industr. Res. Inst. Tokyo,60, No. 2, 37–42 (1965).

  8. 8.

    M. Verzele, J. Chromatogr.,13, 377 (1964).

  9. 9.

    M. Verzele, J. Chromatogr.,19, 504 (1966).

  10. 10.

    M. Verzele, J. Bonche, and M. Verstappe, J. Chromatogr.,18, 253 (1965).

  11. 11.

    M. Verzele, J. Gas Chromatogr.,4, 180, 186 (1966).

  12. 12.

    M. Schingler, Chemistry and Industry, 9, 225 (1960).

  13. 13.

    B.A. Rudenko, V.F. Kucherov, and A.S. Yufut, Transactions of the Conference on Acetylene Chemistry [in Russian], A.A. Petrov (editor), Dushanbe (1968).

  14. 14.

    B.A. Rudenko and V.F. Kucherov, USSR Patent No. 1138478/26-25 (March 9, 1967); Byul. Izobr., No. 17 (1969).

  15. 15.

    V.N. Naukov, Dissertation [in Russian], Moscow (1968).

  16. 16.

    M.Z. Krimer, V.A. Smut, A.V. Semenovskii, and V.F. Kucherov, Izv. Akad. Nauk SSSR, Ser. Khim., 1352 (1968).

  17. 17.

    E.N. Prilezhaeva, R.I. Shekhtman, V.I. Snegotskii, V.N. Lava, and B.A. Rudenko, Izv. Akad. Nauk SSSR, Ser. Khim., 1945 (1970).

  18. 18.

    L.A. Yanovskaya, B.A. Rudenko, and V.F. Kucherov, Izv. Akad. Nauk SSSR, Ser. Khim., 2182, 2189 (1963).

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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 7, pp. 1384–1390, July, 1971.

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Rudenko, B.A., Kuzovkin, V.A., Paukov, V.N. et al. Preparative gas-liquid chromatography with increased efficiency. Russ Chem Bull 20, 1292–1297 (1971). https://doi.org/10.1007/BF00857375

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Keywords

  • Sodium
  • Chloride
  • Chromatography
  • Sodium Chloride
  • Optimum Condition