The optimum conditions for the preparative gas-chromatographic separation of organic substances with an efficiency of up to 2000 theoretical plates, with a simultaneous load of up to 1–2 g, were developed.
Designs of an accessible preparative chromatograph for the separation of unstable compounds were suggested, and the possibility of using it for the separation of organic substances of various classes was demonstrated.
The promise of the use of sodium chloride as the solid phase for the preparative gas-chromatographic separation of unstable compounds was demonstrated.
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Rudenko, B.A., Kuzovkin, V.A., Paukov, V.N. et al. Preparative gas-liquid chromatography with increased efficiency. Russ Chem Bull 20, 1292–1297 (1971). https://doi.org/10.1007/BF00857375
- Sodium Chloride
- Optimum Condition