A method has been developed for GLC analysis of the reaction mixture formed by the vinylation of triethanolamine; the method can be used while carrying out the processes of synthesis and separation of the vinyl ethers of triethanolamine.
By combining the chemical and GLC analysis of this reaction mixture the presence of anomalous products of the conversion of triethanolamine under vinylation conditions has been demonstrated; these products are the mono- and divinyl ethers of diethanolamine and the vinyl ether of N-hydroxyethylmorpholine; the total content of these is 14–20% and is dependent on the conditions for carrying out the process.
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Ostrovskii, S.A., Ustynyuk, L.A., Kononov, N.F. et al. Conversion products from triethanolamine under vinylation reaction conditions and their analysis. Russ Chem Bull 19, 1990–1992 (1970). https://doi.org/10.1007/BF00849788
- Total Content
- Vinyl Ether