The reaction of poly- and perfluoroaldehyde hydrazones with hydrazine hydrate was studied. A new preparative method for obtaining the hitherto inaccessibleN,N-unsubstituted bis-hydrazones of polyfluorinated α-oxoaldehydes was developed based on this reaction.
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Yu. N. Kitaev and B. I. Buzykin,Gidrazony [Hydrazones], Nauka, Moscow, 1974 (in Russian).
I. L. Knunyants and M. D. Bargamova,Izv. Akad. Nauk SSSR, Ser. Khim., 1977, 1916 [Bull. Acad. Sci. USSR, Div. Chem. Sci., 1977,26 (Engl. Transl.)].
For Part 2, seeIzv. Akad. Nauk, Ser. Khim., 1995, 2465 [Russ. Chem. Bull, 1995,44, 2360 (Engl. Transl.)].
Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 12, pp. 2526–2527, December, 1995.
This study was financially supported by the Russian Foundation for Basic Research (Grant No. 94-03-08548) and the International Science Foundation (Grant Nos. NDL 000 and NDL 300).
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Bargamov, G.G., Bargamova, M.D. Polyfluorinated hydrazones in organic syntheses. Russ Chem Bull 44, 2422–2423 (1995). https://doi.org/10.1007/BF00713619
- hydrazine hydrate
- poly- and perfluoroaldehyde hydrazones
- polyfluorinated α-oxoaldehyde bis-hydrazones