The reactions of 2-dimethylamino-, 2-methoxy-, 2-chloro-4,5-dimethyl-1,3,2-dioxaphos-pholanes with 4-thiocyanato-2-butanol in all cases yield 2-(1-methyl-3-thiocyanatopropoxy)-4,5-dimethyl-1,3,2-dioxaphospholane. The latter reacts with elemental sulfur to form the corresponding thiophosphate.
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O. N. Nuretdinova, V. G. Novikova, and L. B. Troitskaya,Izv. Akad. Nauk., Ser. Khim., 1992, 2673 [Bull. Russ. Acad. Sci., Div. Chem. Sci., 1992,41, 2119 (Engl. Transl.)].
O. N. Nuretdinova, V. G. Novikova, and F. F. Guseva,Izv. Akad. Nauk., Ser. Khim., 1992, 2834 [Bull. Russ. Acad. Sci., Div. Chem. Sci., 1992,41, 2241 (Engl. Transl.)].
Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 12, pp. 2130–2131, December, 1993.
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Nuretdinova, O.N., Novikova, V.G. Reactions of 1,3,2-dioxaphospholane derivatives with thiocyanatoalcohols. Russ Chem Bull 42, 2043–2044 (1993). https://doi.org/10.1007/BF00698895
- 2-dimethylamino-, 2-methoxy-, 2-chloro-4,5-dimethyl-1,3,2-dioxaphospholanes