The X-ray structure of the 1,4-butanediol clathrate ofN,N′-[1,3-azulenylenebis(methylene)]bis(trimethyl-ammonium)-diiodide is described, and the differences as well as the similarities to the 1-butanol inclusion of the same host are discussed in detail. The unit cell data of further clathrates of this new type are quoted.
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F. Vögtle, H.-G. Löhr, H. Puff and W. Schuh,Angew. Chem. 95, 425 (1983);Angew. Chem., Int. Ed. Engl. 22, 409 (1983);Angew. Chem. Suppl. 1983, 527–536.
H.-G. Löhr, F. Vögtle, W. Schuh and H. Puff,J. Chem. Soc. Chem. Commun. 924 (1983).
E. Weber and H.-P. Josel,J. Incl. Phenom. 1, 79 (1983).
The lattice parameters were determined from single crystals by least squares refinement of the positions of 25 reflexions.
Supplementary Data. Details of the crystal structure are available on request from the Fachinformationszentrum Energie-Physik-Mathematik, D-7515 Eggenstein, Leopoldshafen 2, by quoting the depository number CSD50482, the names of the authors, and the journal citation
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Löhr, H., Vögtle, F., Schuh, W. et al. The structure of the 1,4-butanediol clathrate of a bis-ammonium salt of azulene. Journal of Inclusion Phenomena 1, 175–179 (1983). https://doi.org/10.1007/BF00656820
- X-ray analysis
- onium compounds
- azulene derivative