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Journal of Materials Science

, Volume 28, Issue 19, pp 5237–5239 | Cite as

Microstructural development and sintering of NdFeB alloys

  • M. R. Nasseri Pouryazdi
  • G. W. Johnson
  • A. J. Moulson
Papers

Abstract

The reactions and phase changes occurring during sintering of NdFeB permanent magnet alloys were studied by differential thermal analysis and scanning electron microscopy. The powders were produced by hydrogen decrepitation and on heating, hydrogen evolution occurred in two stages: firstly from the matrix phase (∼170 °C) and then from the neodymium-rich phase (350–750 °C). The neodymium-rich phase melted at ∼630 °C and no significant microstructural changes occurred below this temperature. Above 630 °C the neodymium phase is mobile, wetting the matrix grains and leading to their magnetic isolation. Densification occurs by a solution/precipitation mechanism.

Keywords

Hydrogen Polymer Scanning Electron Microscopy Thermal Analysis Phase Change 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Copyright information

© Chapman & Hall 1993

Authors and Affiliations

  • M. R. Nasseri Pouryazdi
    • 1
  • G. W. Johnson
    • 1
  • A. J. Moulson
    • 1
  1. 1.School of MaterialsUniversity of LeedsLeedsUK

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