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Dimerization of 9-isopropenyl phenanthrene by TiCl4

Structural study of the dimer

Summary

9-isopropenyl phenanthrene was dimerized by reaction with TiCl4, in CH2Cl2 and the structure of the dimer studied by 1H NMR spectroscopy. The structure results from the attack of carbocation on carbon 9.

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References

  1. BARTHE K.D. and SMITH J.A.S.: Spectrochim. Acta, 23A, 1689 (1967)

  2. BAVIN P.M.G., BARTHE K.D. and SMITH J.A.S.: Tetrahedron, 21, 1087 (1965)

  3. BUNEL C., BRIGODIOT M. and MARECHAL E.: J. Macromol. Sci. : Chem., (in press)

  4. COUDANE J., BRIGODIOT M. and MARECHAL E.: Polymer Bulletin, Preceeding articles

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Coudane, J., Brigodiot, M. & Marechal, E. Dimerization of 9-isopropenyl phenanthrene by TiCl4 . Polymer Bulletin 1, 475–479 (1979). https://doi.org/10.1007/BF00255711

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Keywords

  • Polymer
  • Spectroscopy
  • CH2Cl2
  • Material Processing
  • Phenanthrene