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Synthesis and crystal structure of [Cr(NH3)5Cl][PdCl4]·H2O

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Abstract

Synthesis and investigation of a binary complex salt [Cr(NH3)5Cl][PdCl4]·H2O is reported. The compound is isostructural with [Rh(NH3)5Cl][PdCl4]·H2O studied earlier; it was characterized by element analysis and powder and single crystal X-ray diffraction. Crystal data for H17Cl5N5OPdCr: a = 7.8668(12) Å, b = 10.9703(16) Å, c = 16.048(2) Å, β = 102.469(3)°, space group P21/c, Z = 4, V = 1352.3(3)Å3, d calc = 2.155 g/cm3.

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Authors and Affiliations

  1. A. V. Nikolaev Institute of Inorganic Chemistry, Russian Academy of Sciences, Siberian Branch, Novosibirsk

    I. A. Baidina, P. E. Plyusnin, S. V. Korenev, K. V. Yusenko, Yu. V. Shubin & S. A. Gromilov

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  1. I. A. Baidina
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  2. P. E. Plyusnin
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  3. S. V. Korenev
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  4. K. V. Yusenko
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  5. Yu. V. Shubin
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  6. S. A. Gromilov
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Original Russian Text Copyright © 2004 by I. A. Baidina, P. E. Plyusnin, S. V. Korenev, K. V. Yusenko, Yu. V. Shubin, and S. A. Gromilov

Translated from Zhurnal Strukturnoi Khimii, Vol. 45, No. 3, pp. 549–552, May–June 2004.

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Baidina, I.A., Plyusnin, P.E., Korenev, S.V. et al. Synthesis and crystal structure of [Cr(NH3)5Cl][PdCl4]·H2O. J Struct Chem 45, 523–526 (2004). https://doi.org/10.1007/s10947-005-0023-8

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  • DOI: https://doi.org/10.1007/s10947-005-0023-8

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